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Methods: Potentiometric nonaqueous titrations(potentionmetry) and nonaqueous titrations of malachite green indicator(indicator method) were adopt. 方法:采用非水電位滴定法(以下簡(jiǎn)稱電位法)和以孔雀綠為指示劑的非水滴定法(以下簡(jiǎn)稱指示劑法)。